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ISO 3924:2019 specifies a method for the determination of the boiling range distribution of petroleum products. The method is applicable to petroleum products and fractions with a final boiling point of 538 °C or lower at atmospheric pressure as determined by this document. This document does not apply to gasoline samples or gasoline components. The method is limited to products having a boiling range greater than 55 °C and having a vapour pressure sufficiently low to permit sampling at ambient temperature.

The document describes two procedures.

a) Procedure A allows a larger selection of columns and analysis conditions, such as packed and capillary columns as well as a thermal conductivity detector in addition to the flame ionization detector. Analysis times range from 14 min to 60 min.

b) Procedure B is restricted to only three capillary columns and requires no sample dilution. The analysis time is reduced to about 8 min.

Both procedures have been successfully applied to samples containing fatty acid methyl esters (FAME) up to 20 % (volume fraction).

NOTE For the purposes of this document, the terms "% (mass fraction)" and "% (volume fraction)" are used to represent the mass fraction (°), the volume fraction (φ) of a material.

 

Document History

  1. ISO 3924:2019

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    Petroleum products - Determination of boiling range distribution - Gas chromatography method

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  2. ISO 3924:2016


    Petroleum products - Determination of boiling range distribution - Gas chromatography method

    • Historical Version
  3. ISO 3924:2010


    Petroleum products - Determination of boiling range distribution - Gas chromatography method

    • Historical Version
  4. ISO 3924:1999


    Petroleum products -- Determination of boiling range distribution -- Gas chromatography method

    • Historical Version